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HRID35073

反应详情

EQUATION

反应方程式

HRID 35073 的结构方程式

REACTANTS

反应物

2
结构：CCCCCCCCCCN1C(=O)C2CC(c3ccc([N+](=O)[O-])cc3)(C2)C1=O
HCID14872616

未命名化合物

结构：CCCCCC.CCOC(C)=O
HCID21226206

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCCCN1C(=O)C2CC(c3ccc(N)cc3)(C2)C1=O
HCID14872623

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：COCCO
溶剂HCID8019

2-Methoxyethanol

C3H8O2

PROCEDURE

实验过程

In a manner analogous to that described in Example 1a, 6.0 g of 3-n-decyl-1-(4-nitrophenyl)-3-azabicyclo[3.1.1]heptane-2,4-dione are dissolved in 120 ml of 2-methoxyethanol, hydrogenated in the presence of 0.6 g of 5% palladium-on-carbon and worked up. Melting point 81.5°-82.5° (from ethyl acetate/hexane).