HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-4-fluorobenzenesulphonyl chloride → HCID 178513461, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-4-fluorobenzenesulphonyl chloride | HCID 145222 | — |
| Reactant | 4-Chlorobenzene-1-carboximidamide hydrochloride | HCID 203436 | — |
| Product | HCID 178513461 | HCID 178513461 | — |
Reaction Steps
4-chlorobenzamidine hydrochloride (0.025 g, 0.133 mmol) and 3-chloro-4 fluorophenyl sulfonylchloride (0.0304 g, 0.133 mmol); were used essentially as described in Example 114 to prepare the title compound. ES Positive Ion MS [M+H]+ ions observed: m/z 347 (35Cl, 35Cl), m/z 349 (37Cl, 37Cl) and m/z 351 (37Cl, 37Cl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07183320B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-de2086c618724f19854538d46869cde7 |
| Source note | uspto-grants-2007_02 |