Thionyl Chloride → HCID 21917114, compound

HRID 351138Notes

Reaction equation

HRID 351138 reaction equation
[C:1]1([CH2:7][C:8]([NH:10][CH2:11][CH2:12][C:13]2[CH:14]=[CH:15][CH:16]=[C:17]3[C:22]=2[CH:21]=[C:20]([C:23]([OH:25])=O)[CH:19]=[CH:18]3)=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.S(Cl)([Cl:28])=O>>[C:1]1([CH2:7][C:8]([NH:10][CH2:11][CH2:12][C:13]2[CH:14]=[CH:15][CH:16]=[C:17]3[C:22]=2[CH:21]=[C:20]([C:23]([Cl:28])=[O:25])[CH:19]=[CH:18]3)=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 21917125HCID 21917125, compound

Product 1

HCID 21917114HCID 21917114, compound

Procedure

5 mmol of the product obtained in Step C are dissolved in 40 ml of thionyl chloride. After stirring under an inert atmosphere for 1 hour, the thionyl chloride is evaporated off under reduced pressure to yield the title product.

Workup

  1. customthe thionyl chloride is evaporated off under reduced pressure

Sources & evidence

ORD record
ord-6250fc7b6e444804a5238959ef3e06ca
Source dataset
uspto-grants-2007_02
Patent number
US07183318B2

Reaction notes

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