HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 21091115, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 21090872 | HCID 21090872 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 21091115 | HCID 21091115 | — |
Reaction Steps
To a solution of 4-[1-(4-methoxyphenyl)-3-(trifluoromethyl)-1H-pyrazol-5-yl]benzylamine hydrochloride obtained by Example 57 (100 mg) and triethylamine (0.073 ml) in chloroform (10 ml) was added dropwise methanesulfonyl chloride (0.04 ml) at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07183306B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-f3c1c38dfd434e15b8a37d213ee82d47 |
| Source note | uspto-grants-2007_02 |