HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 21091138, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 21090957 | HCID 21090957 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21091138 | HCID 21091138 | — |
Reaction Steps
To a solution of 4-[5-(4-methoxyphenyl)-3-(trifluoromethyl)-1H-pyrazol-1-yl]benzylamine hydrochloride obtained by Example 70 (150 mg) and triethylamine (0.1 ml) in dichloromethane (10 ml) was added dropwise methanesulfonyl chloride (0.06 ml) under ice cooling.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07183306B2 |
| Source dataset | uspto-grants-2007_02 |
| ORD ID | ord-bae1a2521d55490c81a698c536a80e43 |
| Source note | uspto-grants-2007_02 |