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Methyl perfluorobutyl ether → Butane, 1-(chloromethoxy)-1,1,2,2,3,3,4,4,4-nonafluoro-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl perfluorobutyl ether | HCID 164514 | — |
| 反応物 | Butane, 1-(chloromethoxy)-1,1,2,2,3,3,4,4,4-nonafluoro- | HCID 9925852 | — |
| 反応物 | HCID 131724435 | HCID 131724435 | — |
| 生成物 | Butane, 1-(chloromethoxy)-1,1,2,2,3,3,4,4,4-nonafluoro- | HCID 9925852 | — |
| 生成物 | C4F9OCHCl2 | HCID 9927029 | — |
反応手順
GLC at the conclusion of the addition showed the following C4F9OCH3(5%), C4F9OCH2Cl (65%) and C4F9OCHCl2 HCl2 (29%) and C4F9OCCl3 (0.2%). The reaction solution was washed first with dilute aqueous potassium hydroxide, and then with water, and distilled using a 40-plate perforated plate column to yield C4F9OCH2Cl, b.p.=87° C. and C4F9OCHCl2, b.p.=96° C. in purifies of about 99%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06743262B1 |
| 出典データセット | uspto-grants-2004_06 |
| ORD ID | ord-75b885c6c38e4e7893cd358e501abbe0 |
| 出典メモ | uspto-grants-2004_06 |