HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 351487Generated: October 30, 2026
Methyl Acrylate → HCID 21872363, compound
https://huagongshe.com/reaction/351487
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | 2-Methoxyethylamine | HCID 8018 | — |
| Reactant | Bromoacetonitrile | HCID 11534 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 21872363 | HCID 21872363 | — |
Reaction Steps
At 20 to 30° C., 11.4 g of methyl acrylate was added to 10.0 g of 2-methoxyethylamine, which was allowed to stand for 2 hours. Then 7.92 g of bromoacetonitrile was added to the reaction solution, which was heated at 70° C. for 20 hours. The reaction solution was diluted with ethyl acetate and the resulting solids were filtered off. Vacuum concentration yielded methyl N-cyanomethyl-N-(2-methoxy-ethyl)-3-aminopropionate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06743564B2 |
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| Source dataset | uspto-grants-2004_06 |
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| ORD ID | ord-a7a0d27e20f34500b109162c6849e0dc |
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| Source note | uspto-grants-2004_06 |
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