HCID 21872330, compound → HCID 21872593, compound

HRID 351488Notes

Reaction equation

HRID 351488 reaction equation
[C:1]([CH2:3][N:4]([CH2:11][CH2:12][OH:13])[CH2:5][CH2:6][C:7]([O:9][CH3:10])=[O:8])#[N:2].[C:14](OCCN(C#N)CC(C)C(OC)=O)(=[O:16])[CH3:15]>>[C:14]([O:13][CH2:12][CH2:11][N:4]([CH2:3][C:1]#[N:2])[CH2:5][CH2:6][C:7]([O:9][CH3:10])=[O:8])(=[O:16])[CH3:15]

Participants

3

Reactant 2

HCID 21872330HCID 21872330, compoundHCID 86585653HCID 86585653, compound

Product 1

HCID 21872593HCID 21872593, compound

Procedure

By following the same procedure as Synthesis Example 3 except that methyl N-cyanomethyl-N-(2-hydroxyethyl)-3-aminopropionate was used instead of N,N-bis(2-hydroxyethyl)-3-aminopropiononitrile, methyl N-(2-acetoxyethyl)-N-cyano-methyl-3-aminopropionate was synthesized.

Workup

  1. customwas synthesized

Sources & evidence

ORD record
ord-9fbe28d2cfd04b9983dab70b486de639
Source dataset
uspto-grants-2004_06
Patent number
US06743564B2

Reaction notes

Loading…