1-Decanol → HCID 86587064, compound

Participants

Reaction Steps

To ethyl (2RS) (+/−) 2-ethoxy-3-(4-hydroxyphenyl)propanoate (5 mg) in solution in heptane (dried on 4 Å molecular sieves) (1 ml), triethylamine (0.4 μl) and n-decanol (8 μl), were added 4 Å molecular sieves and Rhizopus arrhizus lipase (Fluka 62305; 2.2 U/g) (20 mg). The reaction mixture was shaken at room temperature and analysed at different times. The reaction mixtures were analysed by the gradient HPLC method 2 and by the chiral HPLC method 4.

Provenance & Evidence