HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Decanol → HCID 86587064, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Decanol | HCID 8174 | — |
| Reactant | Ethyl 2-ethoxy-3-(4-hydroxyphenyl)propanoate | HCID 11791243 | — |
| Solvent | Heptane | HCID 8900 | — |
| Product | HCID 86587064 | HCID 86587064 | — |
Reaction Steps
Ethyl (2RS) (+/−) 2-ethoxy-3-(4-hydroxyphenyl)propanoate (5 mg) was added to a solution containing Mucor miehei lipase Lipozym IM (immobilised Mucor miehei lipase commercially available from Novo Nordisk) (10 mg), n-decanol 8 μl, heptane 0.5 ml and 4 Å molecular sieves. The reaction mixture was shaken at room temperature and analysed at different times. The reaction mixtures were analysed by the gradient HPLC method 2 and by the chiral HPLC method.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06743608B2 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-6cbad0705f2848c08e9e31050d43c3f7 |
| Source note | uspto-grants-2004_06 |