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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 351545Generated: October 30, 2026

Hydrazine hydrate (1:1) → HCID 22713193, compound

https://huagongshe.com/reaction/351545

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrazine hydrate (1:1)HCID 24654—
ReactantHCID 22713206HCID 22713206—
SolventEthanolHCID 702—
ProductHCID 22713193HCID 22713193—

Reaction Steps

To a solution of methyl 3-(4-n-hexyloxyphenyl)propionate (1.18 g) in ethanol (10 ml) was added hydrazine monohydrate (1.08 ml) and the mixture was refluxed for 24 hours. After cooling, the solvent was removed under reduced pressure. Water was added and the precipitate was collected by filtration, washed with water and dried under reduced pressure to give 3-(4-n-hexyloxyphenyl)propionohydrazide (0.92 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06743776B2
Source datasetuspto-grants-2004_06
ORD IDord-9019acc141274847aec811ce9e411471
Source noteuspto-grants-2004_06