HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Propanol → propyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Propanol | HCID 1031 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 5,7-dihydro-6H-dibenz[c,e]azepine-6carbonitrile | HCID 19833886 | — |
| Product | propyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate | HCID 19833889 | — |
Reaction Steps
starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and sodium propylate in n-propanol there is obtained propyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and therefrom with hydrochloric acid in alcohol there is obtained the hydrochloride, m.p. 147° C. (with decomposition);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04766115 |
| Source dataset | uspto-grants-1988_08 |
| ORD ID | ord-41cfad21d79044728afd11437251a9db |
| Source note | uspto-grants-1988_08 |