HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanol → cyclohexyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanol | HCID 7966 | — |
| Reactant | 5,7-dihydro-6H-dibenz[c,e]azepine-6carbonitrile | HCID 19833886 | — |
| Product | cyclohexyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate | HCID 20041718 | — |
Reaction Steps
starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and cyclohexanol there is obtained cyclohexyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate as a syrup, 1H-NMR(CDCl3): 1.5-2.1 (8H), 4.2 (s, 4H), 4.67 (broad s, NH), 5.1 (m, OCH), 7.3-7.7 (8H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04766115 |
| Source dataset | uspto-grants-1988_08 |
| ORD ID | ord-d86ea385bc984b039dc781fd12477b0e |
| Source note | uspto-grants-1988_08 |