HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 15612244, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 2-(3-Pyridylmethyl)-6-(2-methyl-1,3-dioxolan-2-yl)naphthalene | HCID 15612243 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 15612244 | HCID 15612244 | 101.3% |
Reaction Steps
A solution of 150 mg of 2-(3-pyridylmethyl)-6-(2-methyl-1,3-dioxolan-2-yl)naphthalene in 15 ml of 1N hydrochloric acid was allowed to stand for 3 hours at room temperature. The solution was neutralized with sodium carbonate and extracted with methylene chloride. The organic layer was dried over sodium sulfate and the solvent removed under reduced pressure to give 130 mg of 2-(3-pyridylmethyl)-6-acetylnaphthalene as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04766127 |
| Source dataset | uspto-grants-1988_08 |
| ORD ID | ord-d087129627ad4ec4a8be14aecff590ba |
| Source note | uspto-grants-1988_08 |