HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lauric Acid → N-(2-Methoxy-5-pyridyl)-cyclopropane carboxamide dodecanoic acid salt
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lauric Acid | HCID 3893 | — |
| Reactant | N-(6-methoxypyridin-3-yl)cyclopropanecarboxamide | HCID 86308 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | N-(2-Methoxy-5-pyridyl)-cyclopropane carboxamide dodecanoic acid salt | HCID 14304482 | — |
Reaction Steps
Three grams (0.016 mole) of the compound of Example 1 was dissolved in 100 ml of acetone in a 300 ml, one-neck, round-bottom flask by swirling. 3.2 g (0.016 mole) dodecanoic acid was added which went into solution. The resulting solution was evaporated on a rotary evaporator, yielding 6.2 g, of a white solid having a melting point of 92°-96° C., which was identified by nuclear magnetic resonance spectroscopy as the title compound. This compound will be known as Compound 7.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04766134 |
| Source dataset | uspto-grants-1988_08 |
| ORD ID | ord-e933d83f36084de3b604fe6075716b29 |
| Source note | uspto-grants-1988_08 |