HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-6-methylpyridine → 4-(6-Methylpyridin-2-yl)-1-naphthoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-6-methylpyridine | HCID 79205 | — |
| Reactant | Methyl 4-(trimethylstannyl)-1-naphthoate | HCID 22711864 | — |
| Product | 4-(6-Methylpyridin-2-yl)-1-naphthoic acid | HCID 22711846 | — |
Reaction Steps
The title compound was prepared from D7 and 2-bromo-6-methylpyridine using a similar method to Description 8 (45%), followed by hydrolysis of the methyl ester using 1M NaOH solution (69%) to afford a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06747030B1 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-0a95f086280d451b9d311771a522dfab |
| Source note | uspto-grants-2004_06 |