Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tert-butyl 4-benzylpiperazine-1-carboxylate → 1-Benzylpiperazine hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tert-butyl 4-benzylpiperazine-1-carboxylate | HCID 584330 | — |
| 반응물 | Ethanol hydrochloride | HCID 21887872 | — |
| 생성물 | 1-Benzylpiperazine hydrochloride | HCID 2756653 | 97% |
반응 단계
To 1-benzyl-4-tert-butoxycarbonylpiperazine (3.12 g), saturated ethanol hydrochloride was added, followed by stirring for 90 minutes at room temperature. The solvent was distilled off under reduced pressure, followed by drying, whereby the title compound (2.73 g, 97%) was obtained as white powder.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06747023B1 |
| 출처 데이터셋 | uspto-grants-2004_06 |
| ORD ID | ord-33705c0319e7456583203d04feae1405 |
| 출처 메모 | uspto-grants-2004_06 |