HCID 22709560, compound → HCID 22710360, compound

HRID 352908Notes

Reaction equation

HRID 352908 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][C:11]=1[C:12]1[CH:17]=[CH:16][N:15]=[CH:14][CH:13]=1)[C:6]([OH:8])=O.Cl.[Cl:19][C:20]1[CH:21]=[C:22]2[C:27](=[CH:28][CH:29]=1)[CH:26]=[C:25]([S:30]([N:33]1[CH2:38][CH2:37][NH:36][CH2:35][CH2:34]1)(=[O:32])=[O:31])[CH:24]=[CH:23]2>>[ClH:19].[Cl:19][C:20]1[CH:21]=[C:22]2[C:27](=[CH:28][CH:29]=1)[CH:26]=[C:25]([S:30]([N:33]1[CH2:34][CH2:35][N:36]([C:6](=[O:8])[C:5]3[CH:9]=[CH:10][C:11]([C:12]4[CH:17]=[CH:16][N:15]=[CH:14][CH:13]=4)=[C:3]([O:2][CH3:1])[CH:4]=3)[CH2:37][CH2:38]1)(=[O:31])=[O:32])[CH:24]=[CH:23]2

Participants

3

Reactant 2

HCID 22709560HCID 22709560, compoundHCID 227097661-(6-Chloronaphth-2-ylsulphonyl)piperazine hydrochloride

Product 1

HCID 22710360HCID 22710360, compound

Procedure

In the same manner as in Example A-4, a reaction was conducted using 3-methoxy-4-(4-pyridyl)benzoic acid and 1-[(6-chloronaphthalen-2-yl)sulfonyl]piperazine hydrochloride as starting materials, whereby the title compound was obtained.

Sources & evidence

ORD record
ord-7aac636e473d4c4e8e42c3cb62498f49
Source dataset
uspto-grants-2004_06
Patent number
US06747023B1

Reaction notes

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