HCID 22710999, compound → HCID 22710501, compound
Reaction equation
[CH3:1][CH:2]1[NH:7][CH2:6][C:5]2[S:8][C:9]([C:11]([O-:13])=O)=[N:10][C:4]=2[CH2:3]1.[Li+].[Cl:15][C:16]1[CH:17]=[C:18]2[C:23](=[CH:24][CH:25]=1)[CH:22]=[C:21]([S:26]([N:29]1[CH2:34][CH2:33][NH:32][CH:31]([C:35](=[O:41])[NH:36][CH2:37][CH2:38][O:39][CH3:40])[CH2:30]1)(=[O:28])=[O:27])[CH:20]=[CH:19]2>>[ClH:15].[Cl:15][C:16]1[CH:17]=[C:18]2[C:23](=[CH:24][CH:25]=1)[CH:22]=[C:21]([S:26]([N:29]1[CH2:34][CH2:33][N:32]([C:11]([C:9]3[S:8][C:5]4[CH2:6][NH:7][CH:2]([CH3:1])[CH2:3][C:4]=4[N:10]=3)=[O:13])[CH:31]([C:35](=[O:41])[NH:36][CH2:37][CH2:38][O:39][CH3:40])[CH2:30]1)(=[O:27])=[O:28])[CH:20]=[CH:19]2Participants
3
Procedure
Starting materials: lithium 6-methyl-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine-2-carboxylate, 4-[(6-chloronaphthalen-2-yl)sulfonyl]-2-[[N-(2-methoxyethyl)]carbamoyl]piperazine
Sources & evidence
- ORD record
- ord-52ecc670f6c448c69397a86cc1a1433b
- Source dataset
- uspto-grants-2004_06
- Patent number
- US06747023B1
Reaction notes
Loading…