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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 353019Generated: October 26, 2026

Methyl p-toluenesulfonate → 3-Methyl-6-nitrobenzothiazolium p-toluenesulfonate

https://huagongshe.com/reaction/353019

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl p-toluenesulfonateHCID 6645—
Reactant6-NitrobenzothiazoleHCID 76256—
Product3-Methyl-6-nitrobenzothiazolium p-toluenesulfonateHCID 2270687854.1%

Reaction Conditions

Temperature140 °C

Reaction Steps

See FIG. 3A. A mixture of 6-nitrobenzothiazole (1 g) and methyl-p-toluenesulfonate (1.2 g) was heated to 140° C. for 20 min. The solid was washed with acetone and filtered to provide a bluish solid (1.1 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06750024B2
Source datasetuspto-grants-2004_06
ORD IDord-5c7d70f5b34143aabb1d7681bfd4a73c
Source noteuspto-grants-2004_06