HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 9968829, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Ethyl 4-[(3,5-dichlorophenyl)sulfanyl]-5-ethyl-1-(2-hydroxyethyl)-1H-pyrazole-3-carboxylate | HCID 10200330 | — |
| Product | HCID 9968829 | HCID 9968829 | — |
Reaction Steps
A mixture of Example 46 (407 mg, 1.05 mmol) and 0.880 ammonia solution was heated at 90° C. in a sealed Reacti-vial (Trade Mark) for 18 hours. The precipitate was filtered off and washed with water (5 ml) to afford the title compound (273 mg) as a white solid, m.p. 214-216° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06750230B2 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-bc16002b460c4999afdc0949773f1713 |
| Source note | uspto-grants-2004_06 |