HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 2781982, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2,4-Dichloroaniline | HCID 11123 | — |
| Reactant | Bromoacetyl bromide | HCID 61147 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 2781982 | HCID 2781982 | 80.4% |
Reaction Steps
This compound was prepared similarly to Example II-11 from 4.2 g of 2,4-dichloroaniline and 5.76 g of bromoacetyl bromide and 2.89 g of triethylamine in methylene chloride. This gave 5.9 g (80.4%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06750236B2 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-51e3e851cc46461e99c548d6ce900a7b |
| Source note | uspto-grants-2004_06 |