Sodium Hydroxide → HCID 69894550, compound

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Reaction Steps

0.015 g (0.03 mmol) of the compound from Example 3-4 is dissolved in 0.5 ml of ethanol and treated with 0.3 ml of 1N aqueous sodium hydroxide solution. The reaction mixture is stirred for another 5 min and then concentrated using a rotary evaporator. The residue is taken up in a little toluene and the solvent is removed under reduced pressure. The product is then dried under reduced pressure for 20 hours. This gives 0.015 g (95.5% of theory) of the title compound.

Provenance & Evidence