HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → Bis(di-p-tolylamino)benzo[a]perylene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Benzenamine, 4-methyl-N-(4-methylphenyl)- | HCID 69293 | — |
| Reactant | Dibromobenzo[a]perylene | HCID 21910019 | — |
| Catalyst | Copper | HCID 23978 | — |
| Solvent | Water | HCID 962 | — |
| Product | Bis(di-p-tolylamino)benzo[a]perylene | HCID 21910029 | — |
Reaction Steps
Then, two equivalents of di-p-tolylamine, potassium carbonate, and copper power were added to the thus obtained dibromobenzo[a]perylene. This mixture stood still for reaction at 200 degrees centigrade for thirty hours. After reactant solution was diluted with water, reactant was extracted by chloroform. Thereafter, the reactant was refined in a conventional manner to thereby obtain bis(di-p-tolylamino)benzo[a]perylene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06753097B2 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-65e4863b74a84f75b8f25ed37ec71346 |
| Source note | uspto-grants-2004_06 |