HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 4-Chloro-1-naphthalenemethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 4-chloronaphthalene-1-carbaldehyde | HCID 230771 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 4-Chloro-1-naphthalenemethanol | HCID 12749144 | — |
Reaction Steps
This compound was prepared in the manner of Step C, Example 1, using 2.1 grams (0.011 mole) of 4-chloronaphthalenecarbaldehye, 70 mL of methanol, 20 mL of THF, and 2 grams (0.054 mole) of sodium borohydride. This preparation differs in that sodium borohydride was used rather than a solution of potassium hydroxide in water. The yield of the title compound was 1.9 grams.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06753429B2 |
| Source dataset | uspto-grants-2004_06 |
| ORD ID | ord-543dfcfc5a2f46cbb701ae5a6e64fe06 |
| Source note | uspto-grants-2004_06 |