1h-imidazole-1-carboxamide → HCID 21978262, compound

HRID 353640Notes

Reaction equation

HRID 353640 reaction equation
Cl.[NH2:2][CH2:3][CH2:4][NH:5][C:6](=[O:15])[O:7][CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1.[N:16]1([C:21](N)=[O:22])[CH:20]=[CH:19][N:18]=[CH:17]1>>[N:18]1([CH2:19][CH2:20][NH:16][C:21]([NH:2][CH2:3][CH2:4][NH:5][C:6](=[O:15])[O:7][CH2:8][C:9]2[CH:10]=[CH:11][CH:12]=[CH:13][CH:14]=2)=[O:22])[CH2:11][CH2:10][CH2:9][CH2:8][CH2:17]1

Participants

3

Reactant 2

HCID 2653011h-imidazole-1-carboxamideHCID 12715871Benzyl N-(2-aminoethyl)carbamate hydrochloride

Product 1

HCID 21978262HCID 21978262, compound

Procedure

Prepared from benzyl 2-aminoethylcarbamate hydrochloride and N-[2-1-piperidinyl)ethyl]-1H-imidazole-1-carboxamide (Preparation 18) by a similar procedure to Preparation 50. The title compound was obtained as a yellow oil.

Workup

  1. customto Preparation 50

Sources & evidence

ORD record
ord-866b8209604840a2901844351b5ef142
Source dataset
uspto-grants-2004_06
Patent number
US06753322B2

Reaction notes

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