HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 353696Generated: October 25, 2026
Thioglycolic Acid → Ethyl 4-carboxymethylsulfenyl-2-chlorobenzoate
https://huagongshe.com/reaction/353696
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thioglycolic Acid | HCID 1133 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Benzoic acid, 2,4-dichloro-, ethyl ester | HCID 42026 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Ethyl 4-carboxymethylsulfenyl-2-chlorobenzoate | HCID 12993801 | — |
Reaction Steps
A mixture containing ethyl 2,4-dichlorobenzoate (10.0 g), potassium carbonate (9.44 g), dimethylformamide (50 ml), and mercaptoacetic acid (3.8 ml) was allowed to react with heat at 80° C. for 4 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06756343B1 |
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| Source dataset | uspto-grants-2004_06 |
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| ORD ID | ord-80dc97ce6d084062a119638e87f00d1a |
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| Source note | uspto-grants-2004_06 |
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