Ethanethiol → HCID 23511302, compound

HRID 353697Notes

Reaction equation

HRID 353697 reaction equation
[CH3:1][CH:2]([O:4][CH:5]1[C:14]2[C:9](=[C:10]([CH3:26])[CH:11]=[C:12]([C:16]([CH:18]3[CH:23](Cl)[CH2:22][CH2:21][CH2:20][C:19]3=[O:25])=[O:17])[C:13]=2[CH3:15])[S:8](=[O:28])(=[O:27])[CH2:7][CH2:6]1)[CH3:3].[C:29]1([SH:35])[CH:34]=[CH:33][CH:32]=[CH:31][CH:30]=1.ClC1C2CCS(=O)(=O)C=2C=CC=1C(C1C(Cl)CCCC1=O)=O.C(S)C>>[CH3:1][CH:2]([O:4][CH:5]1[C:14]2[C:9](=[C:10]([CH3:26])[CH:11]=[C:12]([C:16]([CH:18]3[CH:23]([S:35][C:29]4[CH:34]=[CH:33][CH:32]=[CH:31][CH:30]=4)[CH2:22][CH2:21][CH2:20][C:19]3=[O:25])=[O:17])[C:13]=2[CH3:15])[S:8](=[O:28])(=[O:27])[CH2:7][CH2:6]1)[CH3:3]

Participants

5

Reactant 4

HCID 6343EthanethiolHCID 7969ThiophenolHCID 23511243HCID 23511243, compoundHCID 23511326HCID 23511326, compound

Product 1

HCID 23511302HCID 23511302, compound

Procedure

The target compound was prepared in the same manner as described in Example II-2 except that 4-(2-propyl)oxy-5,8-dimethyl-6-(3-chloro-1-oxocyclohexan-2-yl)carbonylthiochroman-1,1-dioxide and benzenethiol were used instead of 4-chloro-5-(3-chloro-1-oxocyclohexan-2-yl)carbonyl-2,3-dihydrobenzothiophene-1,1-dioxide and ethanethiol, respectively.

Workup

  1. customThe target compound was prepared in the same manner

Sources & evidence

ORD record
ord-378c7ef463f1454892618258dfe37a0a
Source dataset
uspto-grants-2004_06
Patent number
US06756343B1

Reaction notes

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