Benzamide → N-(6-aminohexyl)benzamide

HRID 353842Notes

Reaction equation

HRID 353842 reaction equation
[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][NH2:8].[C:9](N)(=[O:16])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>>[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][NH:8][C:9](=[O:16])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

Participants

3

Reactant 2

HCID 2331BenzamideHCID 16402Hexamethylenediamine

Product 1

HCID 23512662N-(6-aminohexyl)benzamideYield 62%

Procedure

Using the general method of Example 9 Part A, hexamethylenediamine (348.63 g, 3 mol) was reacted with benzamide (121.14 g, 1 mole) to provide 136.5 g of N-(6-aminohexyl)benzamide.

Sources & evidence

ORD record
ord-e768754078864096b8cd3b6601b93dd6
Source dataset
uspto-grants-2004_06
Patent number
US06756382B2

Reaction notes

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