huagongshe.com
HRID35397

反应详情

EQUATION

反应方程式

HRID 35397 的结构方程式

REACTANTS

反应物

2
结构：O=C(CCl)NCO
HCID62466

2-Chloro-N-(hydroxymethyl)acetamide

C3H6ClNO2

结构：CN(C)C=NS(=O)(=O)c1cc(C(C)(C)C)ccc1O
HCID54155563

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)C=NS(=O)(=O)c1cc(C(C)(C)C)cc(CNC(=O)CCl)c1O
HCID53948117

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O=S(=O)(O)O
溶剂HCID1118

Sulfuric acid

H2O4S

PROCEDURE

实验过程

3 g (0.01 mole) of 4-(1,1-dimethylethyl)-2-dimethylaminomethyleneaminosulfonylphenol are dissolved in 30 ml of sulfuric acid, and 1.1 g (0.009 mole) of 2-chloro-N-hydroxymethylacetamide are added. The mixture is stirred for 30 minutes at room temperature and poured into ice water. The product is filtered off with suction and recrystallized from methanol.

WORKUP

后处理

  1. filtrationThe product is filtered off with suction
  2. customrecrystallized from methanol