HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 354024Generated: October 30, 2026
2,2'-Bipyridine → 2,2'-Bipyridine, 1-oxide
https://huagongshe.com/reaction/354024
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2,2'-Bipyridine | HCID 1474 | — |
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2,2'-Bipyridine, 1-oxide | HCID 36463 | — |
Reaction Steps
A solution of 2,2′-bipyridyl (1 mmole) in dichloromethane was treated with m-chloroperoxybenzoic acid (2 mmole) at 0° C., and the reaction mixture was stirred at 25° C. for 2 h. Extraction and chromatography gave 2,2′-bipyridyl-N-oxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06756360B1 |
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| Source dataset | uspto-grants-2004_06 |
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| ORD ID | ord-764803da4b2c4eff8808f18e2bfdc333 |
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| Source note | uspto-grants-2004_06 |
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