Butylamine → 2-Aminomethyl-6-butylsulfamoyl-4-(1,1-dimethylethyl)phenol hydrochloride

HRID 35407Notes

Reaction equation

C([NH:4][CH2:5][C:6]1[CH:11]=[C:10]([C:12]([CH3:15])([CH3:14])[CH3:13])[CH:9]=[C:8]([S:16]([Cl:19])(=[O:18])=[O:17])[C:7]=1[OH:20])(=O)C.[CH2:21]([NH2:25])[CH2:22][CH2:23][CH3:24]>>[ClH:19].[NH2:4][CH2:5][C:6]1[CH:11]=[C:10]([C:12]([CH3:13])([CH3:14])[CH3:15])[CH:9]=[C:8]([S:16](=[O:17])(=[O:18])[NH:25][CH2:21][CH2:22][CH2:23][CH3:24])[C:7]=1[OH:20]

Participants

Reactant 2

HCID 8007Butylamine

HCID 132103492-Acetamidomethyl-6-chlorosulfonyl-4-(1,1-dimethylethyl)-phenol

Product 1

HCID 212969342-Aminomethyl-6-butylsulfamoyl-4-(1,1-dimethylethyl)phenol hydrochloride

Procedure

This compound is prepared analogously to Examples 11 c and 11 d from 2-acetamidomethyl-6-chlorosulfonyl-4-(1,1-dimethylethyl)-phenol and butylamine.

Sources & evidence

ORD record: ord-f6ce2b6828704a7ca2111061ccd36fd8
Source dataset: uspto-grants-1988_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04766241

Reaction notes

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