Diethanolamine → HCID 12994567, compound

Participants

Reaction Conditions

Reaction Steps

2-(2′-Hydroxy-5′-bromomethylphenyl)benzotriazole (3.03 g, 0.01 mole), diethanol amine (3.14 g, 0.03 mole) were dissolved in 100 mL of acetone. The reaction mixture was refluxed with constant stirring at 75° C. for 6 h. The solvent was then removed by rotary evaporation. Crude product was purified using silica gel column chromatography. Product was identified by 1H-NMR.

Provenance & Evidence