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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 354536Generated: October 28, 2026

HCID 86738803, compound → HCID 86738802, compound

https://huagongshe.com/reaction/354536

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86738803HCID 86738803—
CatalystNickelHCID 935—
ProductHCID 86738802HCID 8673880232.8%

Reaction Steps

(2,6-Dimethyl-3-nitrophenyl)methyl cis-3-(2-chloro-3,3,3-trifluoropropenyl)-2,2-dimethylcyclopropanecarboxylate (11.27 grams, 0.028 mole) was hydrogenated over Raney nickel. The product was chromatographed on an alumina column eluted with toluene to give (3-amino-2,6-dimethylphenyl)methyl cis-3-(2-chloro-3,3,3-trifluoropropenyl)2,2-dimethylcyclopropanecarboxylate (3.45 grams) as a liquid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04375476
Source datasetuspto-grants-1983_03
ORD IDord-6723601b60504a8eb2bd24cc9d38f50f
Source noteuspto-grants-1983_03