HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → [2,6-Dimethyl-3-(1-methylethyl)phenyl]methyl cis-3-(2-chloro-3,3,3-trifluoropropenyl)-2,2-dimethylcyclopropanecarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | [2,6-Dimethyl-3-(1-methylethyl)phenyl]methanol | HCID 20437159 | — |
| Reactant | cis-3-(2-Chloro-3,3,3-trifluoropropenyl)-2,2-dimethylcyclopropanecarbonyl chloride | HCID 86737382 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | [2,6-Dimethyl-3-(1-methylethyl)phenyl]methyl cis-3-(2-chloro-3,3,3-trifluoropropenyl)-2,2-dimethylcyclopropanecarboxylate | HCID 86738808 | — |
Reaction Steps
[2,6-Dimethyl-3-(1-methylethyl)phenyl]methanol (0.7 g, 0.004 mole), cis-3-(2-chloro-3,3,3-trifluoropropenyl)-2,2-dimethylcyclopropanecarboxylic acid chloride (0.97 g, 0.004 mole), pyridine (2 ml) and dry toluene (150 ml) were combined to give [2,6-dimethyl-3-(1-methylethyl)phenyl]methyl cis-3-(2-chloro-3,3,3-trifluoropropenyl)-2,2-dimethylcyclopropanecarboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04375476 |
| Source dataset | uspto-grants-1983_03 |
| ORD ID | ord-c3dd93ac93ba4af3b30f1bc01d59e944 |
| Source note | uspto-grants-1983_03 |