Thionyl Chloride → HCID 12698430, compound

HRID 354575Notes

Reaction equation

HRID 354575 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[C:9]1[C:10]([C:15]([OH:17])=O)=[CH:11][CH:12]=[CH:13][CH:14]=1.S(Cl)([Cl:20])=O>>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[C:9]1[C:10]([C:15]([Cl:20])=[O:17])=[CH:11][CH:12]=[CH:13][CH:14]=1

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 2632512-(2-methoxyphenyl)benzoic acid

Product 1

HCID 12698430HCID 12698430, compound

Procedure

2'-Methoxy-[1,1'-biphenyl]-2-carboxylic acid (32 g., 100 mmole) was dissolved in thionyl chloride (40 ml) and the solution was refluxed for 3 hours. The solution was evaporated to provide the title compound.

Workup

  1. temperaturethe solution was refluxed for 3 hours
  2. customThe solution was evaporated

Sources & evidence

ORD record
ord-2b03ae0f9186451a9d0a4cc759599a7b
Source dataset
uspto-grants-1983_03
Patent number
US04375475

Reaction notes

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