Dichloromethane → HCID 53796796, compound

Participants

Reaction Steps

2 drops of dimethylformamide and then 11.2 g (0.095 mol) of thionyl chloride were added to a solution of 16.8 g (0.07 mol) of 2-(1-nonen-1-yl)-3,3-dimethylcyclopropane acid in 80 ml of methylene chloride. The mixture was then boiled under reflux for 1 hour, the solvent is distilled off in vacuo and the residue was distilled in vacuo. 16 g (89% of theory) of 2-(1-nonen-1-yl)-3,3-dimethylcyclopropanecarboxylic acid chloride with a boiling point of 110°/0.5 mm Hg were obtained in this manner.

Provenance & Evidence