HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(o-fluorophenyl)-1,3-dihydro-1,3,3-trimethyl-7-nitro-2H-1,4-benzodiazepin-2-one → HCID 20506186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(o-fluorophenyl)-1,3-dihydro-1,3,3-trimethyl-7-nitro-2H-1,4-benzodiazepin-2-one | HCID 20506156 | — |
| Reactant | 9-chloro-5-(o-chlorophenyl)-1,3-dihydro-1,3,3-trimethyl-7-nitro-2H-1,4-benzodiazepin-2-one | HCID 20506171 | — |
| Solvent | Diethylether hexane | HCID 21584099 | — |
| Product | HCID 20506186 | HCID 20506186 | — |
Reaction Steps
From 3.1 g (0.0082 mol) of 9-chloro-5-(o-chlorophenyl)-1,3-dihydro-3,3-dimethyl-7-nitro-2H-1,4-benzodiazepin-2-one there is obtained, in analogy to the details in paragraph (c) of Example 1, 9-chloro-5-(o-chlorophenyl)-1,3-dihydro-1,3,3-trimethyl-7-nitro-2H-1,4-benzodiazepin-2-one of melting point 121° (ether/n-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04377522 |
| Source dataset | uspto-grants-1983_03 |
| ORD ID | ord-ee696955b62244059770d2b4f66a0a8d |
| Source note | uspto-grants-1983_03 |