HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzothiazolone → HCID 54205109, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzothiazolone | HCID 13625 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Methyl 8-bromooctanoate | HCID 11107373 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54205109 | HCID 54205109 | — |
Reaction Steps
The product is produced as described in example 1 from 3 g. of NaH (80% suspension in mineral oil), 15.1 g. of benzthiazolin-2-one, 200 cc. of DMF, 23.7 g. of 8-bromo-caprylic acid methyl ester and 3 g. NaJ.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04377695 |
| Source dataset | uspto-grants-1983_03 |
| ORD ID | ord-addf4e48275b4874a28b8f3d64b11e27 |
| Source note | uspto-grants-1983_03 |