HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromooctane → HCID 53973628, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromooctane | HCID 8140 | — |
| Reactant | 2-Hydroxy benzimidazole | HCID 11985 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 2150433 | HCID 2150433 | — |
| Reactant | Methyl 8-bromooctanoate | HCID 11107373 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 53973628 | HCID 53973628 | — |
Reaction Steps
The product is produced as described in example 1 from 0.9 g. of NaH (80% suspension in mineral oil), 7.5 g. of 1-octylbenzimidazolin-2-one (produced) by alkylation from benzimidazolin-2-one with bromooctane according to example 8), 100 cc. of DMF, 7.1 g. of 8-bromocaprylic acid methyl ester and 0.9 g. of NaJ. Eluant in chromatographic purification: hexane/ethylacetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04377695 |
| Source dataset | uspto-grants-1983_03 |
| ORD ID | ord-cb6ba25dbe284f008800d616d4b95ef7 |
| Source note | uspto-grants-1983_03 |