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HRID355041

反应详情

EQUATION

反应方程式

HRID 355041 的结构方程式

REACTANTS

反应物

3
结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

结构：O=c1[nH]c2ccccc2n1-c1ccccc1
HCID84657

2H-Benzimidazol-2-one, 1,3-dihydro-1-phenyl-

C13H10N2O

结构：COC(=O)CCCCCCCCCCBr
HCID223913

Methyl 11-bromoundecanoate

C12H23BrO2

PRODUCTS

生成物

1
结构：COC(=O)CCCCCCCCCCn1c(=O)n(-c2ccccc2)c2ccccc21
HCID12961187

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

The product is produced as described in example 1 from 1.3 g. of NaH (80% suspension in mineral oil), 10 g. of 1-phenylbenzimidazolin-2-one, 200 cc. of DMF, 13.3 g. of 11-bromoundecanoic acid methyl ester and 1.3 g. of NaJ. Eluant in chromatographic purification: hexane/ethylacetate.

WORKUP

后处理

  1. customThe product is produced
  2. customEluant in chromatographic purification