Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium hydride → 7-[3-(3-Chlorophenyl)-2-oxo-benzimidazolin-1-yl]-enanthic ethyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | Ethyl 7-chloroheptanoate | HCID 529988 | — |
| 반응물 | 1-(3-Chlorophenyl)-benzimidazolin-2-one | HCID 20191666 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 7-[3-(3-Chlorophenyl)-2-oxo-benzimidazolin-1-yl]-enanthic ethyl ester | HCID 20506944 | — |
반응 단계
The product is produced as described in example 1 from 1.2 g. of NaH (80% suspension in mineral oil), 9.8 g. of 1-(3-chlorophenyl)-benzimidazolin-2-one (produced in usual manners by subjecting N-(3-chlorophenyl)-o-phenylene diamine to reaction of phosgene), 80 cc. of DMF, 7.7 g. of 7-chloroenanthic acid ethyl ester and 1.2 g. of NaJ.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04377695 |
| 출처 데이터셋 | uspto-grants-1983_03 |
| ORD ID | ord-e9c878b2428847d899354acc8b732023 |
| 출처 메모 | uspto-grants-1983_03 |