HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylbenzyl chloride → HCID 12961176, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylbenzyl chloride | HCID 7722 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 8-(2-Oxobenzimidazolin-1-yl)-caprylic acid methyl ester | HCID 12961171 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 12961176 | HCID 12961176 | — |
Reaction Steps
The product is produced as described in example 1 from 0.72 g of NaH (80% suspension in mineral oil), 7 g. of 8-(2-oxo-benzimidazolin-1-yl)-caprylic acid methyl ester, 100 cc. of DMF, 3.4 g. of 4-methylbenzylchloride and 0.72 g. of NaJ. Eluant for chromatographic purification: hexane/ethylacetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04377695 |
| Source dataset | uspto-grants-1983_03 |
| ORD ID | ord-3b01ad5fa3a54456bc40df3868b8241b |
| Source note | uspto-grants-1983_03 |