Sodium Hydroxide → HCID 12961186, compound

HRID 355069Notes

Reaction equation

HRID 355069 reaction equation
C[O:2][C:3](=[O:30])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][N:11]1[C:15]2[CH:16]=[CH:17][CH:18]=[CH:19][C:14]=2[N:13]([CH2:20][C:21]2[CH:26]=[CH:25][C:24]([O:27][CH3:28])=[CH:23][CH:22]=2)[C:12]1=[O:29].[OH-].[Na+]>>[CH3:28][O:27][C:24]1[CH:25]=[CH:26][C:21]([CH2:20][N:13]2[C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=3[N:11]([CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][C:3]([OH:30])=[O:2])[C:12]2=[O:29])=[CH:22][CH:23]=1

Participants

3

Reactant 2

HCID 14798Sodium HydroxideHCID 53681924HCID 53681924, compound

Product 1

HCID 12961186HCID 12961186, compound

Procedure

The product is produced as described in example 22 from 7 g. of 8-[3-(4-methoxybenzyl)-2-oxo-benzimidazolin-1-yl]-caprylic acid methyl ester and 1.4 g. of NaOH. Recrystallization from ether.

Workup

  1. customThe product is produced
  2. customRecrystallization from ether

Sources & evidence

ORD record
ord-13fc09d31acf43959fb05aee0097c7f6
Source dataset
uspto-grants-1983_03
Patent number
US04377695

Reaction notes

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