HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → 4-Nitrothiophene-2-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | 2-Thiophenecarbonitrile | HCID 66087 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | 4-Nitrothiophene-2-carbonitrile | HCID 819044 | — |
Reaction Steps
To a solution of 2-cyanothiophene (10.9 g; 0.1 mol) in 25 ml of acetic anhydride (t=10° C.) are added 9 ml of fuming nitric acid (d=1.49 g/ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04767758 |
| Source dataset | uspto-grants-1988_08 |
| ORD ID | ord-4447b93923aa4c0cb9b0badc742f9fbb |
| Source note | uspto-grants-1988_08 |