HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Ethyl-2-(1,3-dioxan-4-ylmethoxy)benzaldehyde → 4-Ethyl-2-(1,3-dioxan-4-ylmethoxy)phenylmethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Ethyl-2-(1,3-dioxan-4-ylmethoxy)benzaldehyde | HCID 18941614 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-Ethyl-2-(1,3-dioxan-4-ylmethoxy)phenylmethanol | HCID 18941599 | — |
Reaction Steps
Using a Parr hydrogenator, 3.4 grams (0.014 mole) of 4-ethyl-2-(1,3-dioxan-4-ylmethoxy)benzaldehyde in 200 mL of ethanol was hydrogenated in the presence of 5% palladium on carbon for two hours at 50 psi. The yield of subject compound was 2.3 grams, following purification by column chromatography on silica gel. The NMR spectrum was consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USH0001759 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-3caf45db9cce48a39b81f70a4721203c |
| Source note | uspto-grants-1998_11 |