HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18941601, compound → HCID 18941596, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18941601 | HCID 18941601 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18941596 | HCID 18941596 | — |
Reaction Steps
This compound was hydrogenated in the manner of Step (c) of Example 1, using 7.5 grams (0.036 mole) of 4-ethyl-2-(2-methoxyethoxy)benzaldehyde in 200 mL of ethanol in the presence of 10% palladium on carbon. The yield of the subject compound was 1.8 grams, following purification by column chromatography on silica gel. The NMR spectrum was consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USH0001759 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-0b2f96f74c8d4323a2dd751dd64d96db |
| Source note | uspto-grants-1998_11 |