HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Aminobenzoyl)benzoic acid → 5H-Dibenz(b,e)azepine-6,11-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Aminobenzoyl)benzoic acid | HCID 70847 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | 5H-Dibenz(b,e)azepine-6,11-dione | HCID 70836 | 78.7% |
Reaction Steps
A mixture of 2.50 g of 2-aminobenzophenone2'-carboxylic acid in 50 ml of xylene is stirred at reflux for 23 hours. The mixture is filtered to give 1.82 g of the desired product as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05834461 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-c7c6c0d3586c4ff9ae792a5c5bf25d35 |
| Source note | uspto-grants-1998_11 |