HRID355886

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID2800899

2,3-Dimethylbenzoyl chloride

C9H9ClO

结构：Nc1ccc(C(=O)N2Cc3ccccc3Cc3ccccc32)cc1

HCID15410467

未命名化合物

PRODUCTS

生成物

结构：Cc1cccc(C(=O)Nc2ccc(C(=O)N3Cc4ccccc4Cc4ccccc43)cc2)c1C

HCID67623756

未命名化合物

收率 13.4%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

As described for Example 9, 0.628 g (2 mmol) of 5-(4-aminobenzoyl)-6,11-dihydro-5H-dibenz[b,e]azepine is reacted with 0.506 g (3.0 mmol) of 2,3-dimethylbenzoyl chloride in dichloromethane. The product is recrystallized from hexane-dichloromethane to give 0.12 g of crystals, m.p. 138°-142° C.

WORKUP

后处理

customThe product is recrystallized from hexane-dichloromethane