HRID355944
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
The procedure is as above, with dibromododecane and 2-amino-4-para-tolylpyridine, which is synthesized according to Chambron J.Cl. Strasbourg Tetrah. 1987 43 (5) 895/905. The product obtained is purified in the base state on a silica column with a benzene/ethyl acetate mixture. It is reconverted to the hydrobromide with a mixture of ether and an isopropanol solution of hydrogen bromide. It can then be recrystallized.
WORKUP
后处理
- customis synthesized
- customThe product obtained
- customis purified in the base state on a silica column with a benzene/ethyl acetate mixture
- additionIt is reconverted to the hydrobromide with a mixture of ether
- customIt can then be recrystallized