HRID355944

反应详情

EQUATION

反应方程式

HRID 355944 的结构方程式

PROCEDURE

实验过程

The procedure is as above, with dibromododecane and 2-amino-4-para-tolylpyridine, which is synthesized according to Chambron J.Cl. Strasbourg Tetrah. 1987 43 (5) 895/905. The product obtained is purified in the base state on a silica column with a benzene/ethyl acetate mixture. It is reconverted to the hydrobromide with a mixture of ether and an isopropanol solution of hydrogen bromide. It can then be recrystallized.

WORKUP

后处理

  1. customis synthesized
  2. customThe product obtained
  3. customis purified in the base state on a silica column with a benzene/ethyl acetate mixture
  4. additionIt is reconverted to the hydrobromide with a mixture of ether
  5. customIt can then be recrystallized